Synthesis and Characterization of New 1,2,4-Triazole Derivatives Form 2-Naphthol

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Nour Abd Alrazzak
Saadon Abdulla Aowda
Abbas Jasim Atiyah

Abstract

In this work 1,2,4-triazole derivatives were synthesized from [4-(2-hydroxy naphthyl)diazenyl]benzoic acid [N1] then converted to  [4-(2-hydroxy naphthyl)diazenyl] benzoate [N2] which reacted with thiosemicarbazide and then cyclization by using sodium hydroxide. Then different alkyl halides like (methyl iodide, allyl chloride, proprgyl chloride and benzyl chloride) were added to[4-(2-hydroxy naphthyl)diazenyl]-4H-1,2,4-triazole-3-thiol [N4] that led to alkylation of thiol to afforded compounds [N5] – [N8]. These compounds were characterized by the following techniques: FT-IR, and 1H , 13C NMR spectroscopies, and elemental analysis C.H.N.S. The physical properties of prepared compounds were studied.

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How to Cite
[1]
N. Abd Alrazzak, S. A. Aowda, and A. J. Atiyah, “Synthesis and Characterization of New 1,2,4-Triazole Derivatives Form 2-Naphthol”, JUBPAS, vol. 26, no. 6, pp. 234-252, May 2018.
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